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Oxford Instruments Kelvinox Dilution Insert DIL2
DIL2 was aquired in 2006, mainly financed by the
"SNF Förderungsprofessur Michel Kenzelmann".
It is equipped with a weak link, allowing access to the
range 1...2 K without removing the mixture.
Problems with DIL2
- The weak link is too weak. For the first experiments we
will use a simple copper sample holder, and use the sensor
on the mixing chamber.
DIL2 Sample mounting
used in | MA15 | MA11 | MA02 | MA09 |
sample space diameter [mm] | 17.3 | 17.3 | 23.6 | 45 |
max. sample diameter [mm] | 12 | 12 | 18 | 35 |
distance from thread to beam center [mm] adjustable by about +- 10 mm | 40 | 51 | 97 | 194 |
allowed size below beam center [mm] | 64 | 30 | 60 | 24 |
On the mixing chamber, there is a bolt with an M5 thread
(on the sample container a 7 mm deep hole with an M5 thread is needed).
Preparing DIL
Condense Mixture
Remove Mixture
Warming up
Sensor Calibration
The calibration curve in the FemtoPower system from Oxford Instruments
is generic. For more precise values use the table below.
Mix.Ch. | Display | Sample |
0.043 | 0.040 | 0.036 |
0.063 | 0.060 | 0.055 |
0.084 | 0.080 | 0.075 |
0.104 | 0.100 | 0.094 |
0.155 | 0.150 | 0.143 |
0.205 | 0.200 | 0.191 |
0.306 | 0.300 | 0.289 |
0.407 | 0.400 | 0.387 |
0.609 | 0.600 | 0.581 |
0.811 | 0.800 | 0.777 |
1.013 | 1.000 | 0.972 |
1.521 | 1.500 | 1.461 |
2.029 | 2.000 | 1.951 |
3.050 | 3.000 | 2.938 |
4.075 | 4.000 | 3.929 |
5.105 | 5.000 | 4.925 |
Attachments:
dil2Open.jpg
GasHandling.jpg
dil2.jpg
This particular version was published on 17-Aug-2006 08:35:01 UTC by MarkusZolliker.
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