Diff: HEOX

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JSPWiki v2.0.52


Difference between version 18 and version 1:
Line 1 was replaced by lines 1-77
- HEOX is a
+ !Oxford Intruments 3He Sorption Cryostat
+
+ HEOX is a 3He cryostat with a sorption 3He pump. All gas handling is
+ inside the cryostat, there are therefore no tubes to a pump outside.
+
+ After putting into operation, some questions are still open:
+
+ * The sample space has a diameter of about 40 mm. Around this tube,
+ there is 4.5 mm liquid helium. This produces background,
+ especially on inelastic measurements. A [test on TASP|HeoxOnTasp] shows
+ background count rates of the order of 40 counts/min. which seems
+ to be inacceptable.
+
+ * In principle, it should be possible to combine the 3He insert with
+ the MA09 cryomagnet. It is not yet clear, if it really works, and
+ there will also be the problem with the LHe background.
+
+ * For powders, it is not clear if the thermal contact inside the
+ sample container is good enough to ensure the expected sample
+ temperature.
+
+ ''Some test results''
+
+ Hold times:
+
+ |minimum T|0.33 K|22h
+ | |0.5 K|25h
+ | |0.7 K|32h
+
+ LS340 Settings:
+
+ * Sensor A : 1K-pot
+ * Sensor B : Sorb. (thats the cryo pump for the 3He)
+ * Sensor C : 3He-pot Cernox for 1.2K<T<320K
+ * Sensor D : 3He-pot Speer for T<10K
+ * Sorb heater: 34 Ohm
+ * 3He-pot heater: 200 Ohm
+
+ [Inelastic background on TASP|HeoxOnTasp]
+
+ !Operation with two heaters:
+
+ Heox starts up with the second PID loop (Analog Out2) enabled
+ and loop 1 to control the temperature of the Sorb (Ch B)
+
+ The switch on the heater cable allows to operate the Sorb on loop 1 (the main loop) and simultaneously
+ heat the 3He-pot with loop 2 and visa versa.
+
+ For low Temperature experiments <10K it is recommended to use: Sorb = loop1, 3He = loop2 while for higher
+ temperatures Sorb = loop2, 3He = loop1 should be used. ''note:'' for the high temperatur setting the Cernox (channel C)
+ should be used as the primary thermometer
+
+ You can operate the system by regulating the Sorb and the 3He-pot temperature independently (controlmode 0)
+ or by using both heaters cooperatively to control the 3He-pot temperature (controlmode 1) in this case the setpoints
+ for both loops should have the same value.
+
+ __INPORTANT:__ both heaters are disabled if any setpoint is exactly zero. In order to control the Temperature using only
+ 1 heater the other set value should be small (not reachable)
+
+
+ __sea_commands__
+
+ ''tt controlmode <n>'' ...sets control channel of loop 1 to B (n=0) or D (n=01)
+
+ ''tt set2 <n.n>'' ... setpoint of loop 2 in K
+
+ ''tt send pid n:P,I,D'' ... set PID values of loop n (1 or 2)
+
+ ''tt send cset n:<channel>,<unit>,<off/on>,<power enable>'' ...sets the channel (A,B,C,D)
+ which will be used by loop <n>
+ (e.g. tt send cset 2:D,1,1 sets loop 2 to control the 3He-pot heater
+
+ ''tt send pid?n'' query PID settings of loop n
+
+ ''tt send cset?n'' query control settings of loop n
+
+ [helium3a.jpg]

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