Line 1 was replaced by lines 1-77 |
- HEOX is a |
+ !Oxford Intruments 3He Sorption Cryostat |
+ |
+ HEOX is a 3He cryostat with a sorption 3He pump. All gas handling is |
+ inside the cryostat, there are therefore no tubes to a pump outside. |
+ |
+ After putting into operation, some questions are still open: |
+ |
+ * The sample space has a diameter of about 40 mm. Around this tube, |
+ there is 4.5 mm liquid helium. This produces background, |
+ especially on inelastic measurements. A [test on TASP|HeoxOnTasp] shows |
+ background count rates of the order of 40 counts/min. which seems |
+ to be inacceptable. |
+ |
+ * In principle, it should be possible to combine the 3He insert with |
+ the MA09 cryomagnet. It is not yet clear, if it really works, and |
+ there will also be the problem with the LHe background. |
+ |
+ * For powders, it is not clear if the thermal contact inside the |
+ sample container is good enough to ensure the expected sample |
+ temperature. |
+ |
+ ''Some test results'' |
+ |
+ Hold times: |
+ |
+ |minimum T|0.33 K|22h |
+ | |0.5 K|25h |
+ | |0.7 K|32h |
+ |
+ LS340 Settings: |
+ |
+ * Sensor A : 1K-pot |
+ * Sensor B : Sorb. (thats the cryo pump for the 3He) |
+ * Sensor C : 3He-pot Cernox for 1.2K<T<320K |
+ * Sensor D : 3He-pot Speer for T<10K |
+ * Sorb heater: 34 Ohm |
+ * 3He-pot heater: 200 Ohm |
+ |
+ [Inelastic background on TASP|HeoxOnTasp] |
+ |
+ !Operation with two heaters: |
+ |
+ Heox starts up with the second PID loop (Analog Out2) enabled |
+ and loop 1 to control the temperature of the Sorb (Ch B) |
+ |
+ The switch on the heater cable allows to operate the Sorb on loop 1 (the main loop) and simultaneously |
+ heat the 3He-pot with loop 2 and visa versa. |
+ |
+ For low Temperature experiments <10K it is recommended to use: Sorb = loop1, 3He = loop2 while for higher |
+ temperatures Sorb = loop2, 3He = loop1 should be used. ''note:'' for the high temperatur setting the Cernox (channel C) |
+ should be used as the primary thermometer |
+ |
+ You can operate the system by regulating the Sorb and the 3He-pot temperature independently (controlmode 0) |
+ or by using both heaters cooperatively to control the 3He-pot temperature (controlmode 1) in this case the setpoints |
+ for both loops should have the same value. |
+ |
+ __INPORTANT:__ both heaters are disabled if any setpoint is exactly zero. In order to control the Temperature using only |
+ 1 heater the other set value should be small (not reachable) |
+ |
+ |
+ __sea_commands__ |
+ |
+ ''tt controlmode <n>'' ...sets control channel of loop 1 to B (n=0) or D (n=01) |
+ |
+ ''tt set2 <n.n>'' ... setpoint of loop 2 in K |
+ |
+ ''tt send pid n:P,I,D'' ... set PID values of loop n (1 or 2) |
+ |
+ ''tt send cset n:<channel>,<unit>,<off/on>,<power enable>'' ...sets the channel (A,B,C,D) |
+ which will be used by loop <n> |
+ (e.g. tt send cset 2:D,1,1 sets loop 2 to control the 3He-pot heater |
+ |
+ ''tt send pid?n'' query PID settings of loop n |
+ |
+ ''tt send cset?n'' query control settings of loop n |
+ |
+ [helium3a.jpg] |