At line 7 added 17 lines. |
+ |
+ Working with high temperature furnace need great care: |
+ |
+ * the choice of an adequate container: |
+ ** does the sample react with the container? For metallic |
+ samples, please check the phase diagrams of possible allows |
+ which might be created when the sample reacts with the container |
+ or sample stick. |
+ ** is the sample outgasing? It is preferred to work with |
+ either an open container, or with a container connected |
+ to a tube sample stick, allowing to control the atmosphere |
+ from outside. |
+ * the thermocouples have to be fixed well, and the proper |
+ calibration curve has to be selected. |
+ |
+ The picture below shows what might happen, if these rules are not |
+ obeyed. [FurnaceList/moltenSample.jpg] |