Lines 1-4 were replaced by lines 1-7 |
- ||Name||Description ||T-range||sample\\space\\diameter||Thread on stick |
- |[FS]|small furnace |350...700 K |50|M6 female |
- |[FT]|tantalum furnace|500...1400 K|50|M6 female |
- |[FI]|ILL-type furnace|500...1800 K|40|M8 male |
+ ||Name||Description ||T-range||sample\\space\\diameter||max.\\sample\\diameter||Thread on stick| sample length |
+ |[FS]|small furnace |350...700 K |25*| |M6 female| <70 |
+ |[FT]|tantalum furnace|375...1400 K|50|45|M6 female| |
+ |[FI]|ILL-type furnace\\__temporary out of service__|500...1800 K|40|35|M8 male| |
+ |[FFTF]|fast ramping thin film furnace|300...900 K| 10|10|clamped|thinfilm substrate |
+ (*) 50 mm without radiation screen. However, in this mode very large temperature |
+ gradients are expected. |
At line 7 added 26 lines. |
+ |
+ Working with high temperature furnace need great care: |
+ * the choice of an adequate container: |
+ ** does the sample react with the container? For metallic |
+ samples, please check the phase diagrams of possible alloys |
+ which might be created when the sample reacts with the container |
+ or sample stick. |
+ ** is the sample outgasing? It is preferred to work with |
+ either an open container, or with a container connected |
+ to a tube sample stick, allowing to control the atmosphere |
+ from outside. |
+ * the thermocouples have to be fixed well, and the proper |
+ calibration curve has to be selected. |
+ * __never use Cadmium or Indium in a furnace__, even not at relatively 'low' temperatures |
+ |
+ The pictures below shows what might happen, if these rules are not |
+ obeyed. |
+ |
+ [FurnaceList/moltenSample.jpg] |
+ \\Picture 1: Reaction of the sample with the container. |
+ |
+ [FurnaceList/ftCd1.jpg] |
+ [FurnaceList/ftCd2.jpg] |
+ [FurnaceList/ftCd3.jpg] |
+ [FurnaceList/ftCd4.jpg] |
+ \\Picture 2,3,4,5: Molten and condensed Cadmium. |