Diff: CondenseMixtureDIL

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JSPWiki v2.0.52


Difference between version 2 and version 1:
Line 1 was replaced by line 1
- * fill the cold trap with liquid nitrogen and make sure that
+ * Fill the cold trap with liquid nitrogen and make sure that
At line 2 added 53 lines.
+ * Make sure that all tubes are connected correctly
+
+ * On the Variox or Magnet VTI, open the needle valve more than
+ normally in order to fill the pumping volume with some
+ amount of liquid helium. Put "flow" of 20 mbar until the
+ 1 K pot temperature is stable below 3 K. Then close
+ the needle valve until a "flow" of about 10 mbar is reached
+ (the pressure decreases only slowly). Then regulate the
+ valve at about 10 mbar. This value must not be obeyed exactly,
+ the idea behind the needle valve settings is the following:
+ ** A lower flow is better for consumption (a "flow" of more
+ than 10 mbar increase substatnitally the He consumption, but
+ during the process of condensing it might be o.k.).
+ ** The flow should be high enough to hold the 1 K pot temperature
+ low (over long term: about 2 K with the Variox and about 2.5 K
+ with the MA09). During the condensing phase, the 1 K pot temperature
+ might increate to 3.5 K for a short time, when pushing the
+ mixture quickly.
+
+ * Open the 3 valves in the pumping line and the 2 valves in
+ the condenser line.
+ * Open the green valve marked "out" below the dump. The dump is the
+ grey cylinder in the center of the gas handling system rack.
+ * Open valve 9 (while pressing on the black valve button, press
+ RAISE).
+ * The reading on G2 is proportional to the amout of mixture in the
+ dump. It should read something around 660 mbar.
+ * Open valves 1 and 6 (Valve 6 is a motor valve, while pressing
+ the red valve button, press RAISE until a value of 99.9 is shown).
+ * Open a little valve 12A (4.0 % to start).
+ * While the pressure reading on G1 should always be below about 400 mbar,
+ Valve 12A can bae opened gradually, and opened completely, when the
+ reading on G2 drops below 350 mbar.
+
+ * After some time (about 30 min when using the Variox) the pressure on
+ G1 falls below 150 mbar, and it is time to pump out the dump: close
+ valve 9, and open valve 14 for a short time (close it when P1 raises
+ above 50 mbar). As soon as the pressure on P1 drops down, you might open
+ and close valve 14 again, but make sure that the pressure on G1 does
+ not increase above 350 mbar.
+ * At some stage, when opening valve 14, the pressure on P1 does no longer
+ raise above 50 mbar. Leave the valve open until the P1 drops below 0.1.
+ * The temperature in the mixing chamber goes down in steps during the
+ condensation process. It takes some time until the temperatures start
+ to move downwards, and goes then quickly below 1 K. Then it stays there
+ or decreases slowly to about 0.8 K, for about half an hour or more, before
+ going down by more than 0.01 K per minute.
+
+ * Once the temperature has stabilized in the region of 0.1 K or less,
+ the flow on the condenser line might falls below 100 (black display below
+ the valve panel).
+ Setting the still heater to a power of 3-5 mW, the flow can be increased
+ back to about 100, and the temperature should go down more. Good luck!

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